Significance and Use
5.1 The complex shear modulus is an indicator of the stiffness or resistance of asphalt binder to deformation under load. The phase angle is a measure of the relative portion of the response to an applied load that is elastic (recoverable) or viscous (nonrecoverable).
5.2 The test procedure is applicable to measurements in the linear region where the measured modulus and phase angle are independent of the amplitude of the strain.
5.3 The complex modulus and the phase angle are used to calculate performance-related criteria in accordance with Specification D6373 or D8239.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
Scope
1.1 This test method covers the determination of the complex shear modulus and phase angle of asphalt binders when tested in dynamic (oscillatory) shear using parallel plate geometry.
1.2 This test method is intended for determining the linear viscoelastic properties of asphalt binders as required for specification testing and is not intended as a comprehensive procedure for the full characterization of the viscoelastic properties of asphalt binder.
1.3 This standard is appropriate for unaged asphalt binder, conditioned asphalt binder, and asphalt binder recovered from either asphalt mixtures or asphalt emulsions. To keep the language in this standard precise, the term “asphalt binder” is used to refer to the material being tested.
1.4 This procedure is limited to asphalt binders that contain particles with largest dimension less than 250 μm.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and EPA’s website— www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, into your state may be prohibited by state law.
1.7 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
