DD ISO/TS 15338:2009 Surface chemical analysis. Glow discharge Mass spectrometry (GD-MS). Introduction to use
DD ISO/TS 15338 is a Technical Specification which gives guidelines for the operation of glow discharge mass spectrometry (GD-MS) instruments and recommendations for the use of GD-MS. It is intended to be read in conjunction with the instrument manufacturers’ manuals and recommendations.
Contents of DD ISO/TS 15338:
Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Safety
4.1 Use of high-voltage power supply and connection of the instrument
4.2 Use and storage of compressed-gas cylinders
4.3 Handling of cryogenic materials
5 Principle
6 Materials
7 Apparatus
7.1 Ion source
7.2 Mass analyser
7.3 Detector system
7.4 Vacuum system
7.5 Data acquisition and control
8 Samples and sample preparation
8.1 General
8.2 Sample type
8.3 Sample geometry
8.4 Sample preparation for bulk analysis
8.5 Sample preparation for depth profiling
9 Measurement procedures
9.1 System precautions
9.2 Selection of discharge parameters and isotopes
9.3 Presputtering
9.4 Optimizing the ion current
9.5 Analytical set-up
9.6 Data analysis
9.7 Depth profile analysis
9.8 Instrument performance
9.9 Analysis
10 Test report
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